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Beilstein J. Org. Chem. 2016, 12, 1072–1078, doi:10.3762/bjoc.12.101
Graphical Abstract
Scheme 1: Selected benzothiadaiazine 1,1-dioxides with potent biological activities.
Scheme 2: Scope of acetophenones (reaction conditions: 1 (0.33 mmol), 2a (0.3 mmol), DMSO (2 mL), I2 (0.75 eq...
Scheme 3: Scope of 2-aminobenzenesulfonamides (reaction conditions: 1 (0.33 mmol), 2a (0.3 mmol), DMSO (2 mL)...
Scheme 4: Reactions of 2-aminobenzenesulfonamides bearing an alknyl group (reaction conditions: 1 (0.33 mmol)...
Scheme 5: Gram scale reaction between 1a and 2a.
Figure 1: X-ray crystal structure of 4b (CCDC 1444753).
Scheme 6: Control experiment.
Scheme 7: Proposed mechanism.